THE INVESTIGATION OF THE HAFNIUM CARBIDE FORMATION ON THE CARBON-CARBON COMPOSITE MATERIAL IN THE HFCL4‒СH4‒AR SYSTEM


https://doi.org/10.17073/1683-4518-2017-4-44-49

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Abstract

The  first  stage of  the  technique refinement for  the  thin hafnium carbide coatings formation on the  carbon-carbon composition material (CCCM)  is presented in the  article, the   synthesizing  temperature   being  comparatively  low to  reduce the  thermal stress arising in  the  surface. The hafnium carbide coatings formation on the  CCCM surface was  investigated in the  HfCl4-СH4-Ar system at  1050  °C and atmospheric pressure. The rate of the chloride hafnium (IV) sublimation was studied for different gas consumption values.  The   hafnium carbide  particle  size   distribution histograms were built   and   as  a  result the   polydisperse particle  distribution over   the   CCCM  surface  with   two maximums of average diameters 5,4 micrometers and  295 nanometers were established. Ill. 9. Ref. 11. Tab. 3.


About the Authors

S. A. Eremin
ФГАОУ ВО «НИТУ «МИСиС»
Russian Federation


V. N. Anikin
ФГАОУ ВО «НИТУ «МИСиС»
Russian Federation


D. Yu. Sinitsyn
ФГАОУ ВО «НИТУ «МИСиС»
Russian Federation


V. N. Gus'kov
ФГБУН «Институт общей и неорганической химии имени Н. С. Курнакова РАН»
Russian Federation


A. G. Yudin
ФГАОУ ВО «НИТУ «МИСиС»
Russian Federation


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Supplementary files

For citation: Eremin S.A., Anikin V.N., Sinitsyn D.Y., Gus'kov V.N., Yudin A.G. THE INVESTIGATION OF THE HAFNIUM CARBIDE FORMATION ON THE CARBON-CARBON COMPOSITE MATERIAL IN THE HFCL4‒СH4‒AR SYSTEM. NOVYE OGNEUPORY (NEW REFRACTORIES). 2017;(4):44-49. https://doi.org/10.17073/1683-4518-2017-4-44-49

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