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Полые наноструктурные микросферы Ni3Fe, полученные методом спрей-пиролиза
https://doi.org/10.17073/1683-4518-2023-12-32-37
Аннотация
Представлено исследование двухстадийного метода формирования наноструктурированного Ni3Fe. Наноструктурированные полые микросферы Ni3Fe были синтезированы методом ультразвукового распылительного пиролиза (УРП) из смеси водного 10 %-ного раствора нитратов никеля (II) и железа (III). На первом этапе формировались полые микросферы из смеси оксидов Ni и Fe диаметром в интервале 0,5‒10 мкм. Второй этап ― металлизация смеси оксидов Ni и Fe в трубчатой печи в атмосфере водорода. Данные рентгенографии (XRD) конечного продукта показали наличие фазы Ni3Fe и размер кристаллитов, близкий к 40 нм. Сканирующая и просвечивающая электронная микроскопия показала полую морфологию поученных микросфер Ni3Fe. Их стенки были собраны из кристаллитов диаметром 30‒60 нм.
Об авторах
Б. Б. ХайдаровРоссия
к. т. н.
Москва
А. Г. Юдин
Россия
к. т. н.
Москва
Д. С. Суворов
Россия
Москва
Д. В. Кузнецов
Россия
к. т. н.
Москва
Д. В. Лысов
Россия
Москва
И. Н. Бурмистров
Россия
д. т. н.
Москва
Д. Ю. Карпенков
Россия
к. ф.-м. н.
Москва
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Дополнительные файлы
Для цитирования: Хайдаров Б.Б., Юдин А.Г., Суворов Д.С., Кузнецов Д.В., Лысов Д.В., Бурмистров И.Н., Карпенков Д.Ю. Полые наноструктурные микросферы Ni3Fe, полученные методом спрей-пиролиза. Новые огнеупоры. 2023;(12):32-37. https://doi.org/10.17073/1683-4518-2023-12-32-37
For citation: Khaidarov B.B., Yudin A.G., Suvorov D.S., Kuznetsov D.V., Lysov D.V., Burmistrov I.N., Karpenkov D.Y. Hollow nanostructured microspheres Ni3Fe, obtained by spray-pyrolysis. NOVYE OGNEUPORY (NEW REFRACTORIES). 2023;(12):32-37. (In Russ.) https://doi.org/10.17073/1683-4518-2023-12-32-37
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