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About the Authors

A. G. Yudin
ФГАОУ ВО «Национальный исследовательский технологический университет «МИСиС»
Russian Federation

к. т. н.
Москва

D. V. Lysov
ФГАОУ ВО «Национальный исследовательский технологический университет «МИСиС»
Russian Federation

Москва

K. O. Chuprunov
ФГАОУ ВО «Национальный исследовательский технологический университет «МИСиС»
Russian Federation

Москва

D. V. Leibo
ФГАОУ ВО «Национальный исследовательский технологический университет «МИСиС»
Russian Federation

Москва

E. A. Kolesnikov
ФГАОУ ВО «Национальный исследовательский технологический университет «МИСиС»
Russian Federation

Москва

D. V. Kuznetsov
ФГАОУ ВО «Национальный исследовательский технологический университет «МИСиС»
Russian Federation

к. т. н.
Москва

I. A. Ilyinykh
ФГАОУ ВО «Национальный исследовательский технологический университет «МИСиС»
Russian Federation

Москва

The effect of ultrasonic treatment on the phase composition of hydroxylapatite synthesized using a hydrothermal technique

A. G. Yudin, D. V. Lysov, K. O. Chuprunov, D. V. Leibo, E. A. Kolesnikov, D. V. Kuznetsov, I. A. Ilyinykh

https://doi.org/10.17073/1683-4518-2019-10-48-53

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Abstract

The influence of the duration of ultrasonic treatment after hydrothermal synthesis of hydroxylapatite (HA) samples synthesized in the Ca(NO₃)₂‒(NH₄)₂HPO₄‒NH₄OH precursor system on the phase composition and crystallinity of the synthesized samples is considered. HA samples were investigated using X-ray diffraction and infrared Fourier spectroscopy. The study showed that ultrasonic treatment, regardless of the duration, does not affect the phase composition and crystallinity of the obtained HA samples. In all the studied samples, the presence of the HA phase Ca₁₀(PO₄)₆(OH)₂ with a crystallinity of 0,97 was established.

Keywords

hydroxylapatite, hydrothermal synthesis method, ultrasonic treatment, crystallinity, bioceramics,

About the Authors

A. G. Yudin

ФГАОУ ВО «Национальный исследовательский технологический университет «МИСиС»
Russian Federation

D. V. Lysov

ФГАОУ ВО «Национальный исследовательский технологический университет «МИСиС»
Russian Federation

K. O. Chuprunov

ФГАОУ ВО «Национальный исследовательский технологический университет «МИСиС»
Russian Federation

D. V. Leibo

ФГАОУ ВО «Национальный исследовательский технологический университет «МИСиС»
Russian Federation

E. A. Kolesnikov

ФГАОУ ВО «Национальный исследовательский технологический университет «МИСиС»
Russian Federation

D. V. Kuznetsov

ФГАОУ ВО «Национальный исследовательский технологический университет «МИСиС»
Russian Federation

I. A. Ilyinykh

ФГАОУ ВО «Национальный исследовательский технологический университет «МИСиС»
Russian Federation

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Supplementary files

For citation: Yudin A.G., Lysov D.V., Chuprunov K.O., Leibo D.V., Kolesnikov E.A., Kuznetsov D.V., Ilyinykh I.A. The effect of ultrasonic treatment on the phase composition of hydroxylapatite synthesized using a hydrothermal technique. NOVYE OGNEUPORY (NEW REFRACTORIES). 2019;(10):48-53. https://doi.org/10.17073/1683-4518-2019-10-48-53

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